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作者: simonzrh 发布日期: 2008-05-29
作者: 纳米镍粉 发布日期: 2008-05-29
Name and formula
Reference code: 00-042-1467
PDF index name: Cobalt Oxide
Empirical formula: Co3O4
Chemical formula: Co3O4
Crystallographic parameters
Crystal system: Cubic
Space group: Fd-3m
Space group number: 227
a (?): 8.0837
b (?): 8.0837
c (?): 8.0837
Alpha (°): 90.0000
Beta (°): 90.0000
Gamma (°): 90.0000
Calculated density (g/cm^3): 6.05
Volume of cell (10^6 pm^3): 528.24
Z: 8.00
RIR: 3.10
Subfiles and Quality
Subfiles: Inorganic
Alloy, metal or intermetalic
Corrosion
Common Phase
Quality: Star (S)
Comments
Color: Black
General comments: Average relative standard deviation in intensity of the ten strongest reflections for three specimen mounts=4.0%.
Validated by calculated pattern.
Sample source: Sample obtained from Fischer Scientific.
Additional pattern: To replace 00-009-0418.
References
Primary reference: Martin, K., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA., ICDD Grant-in-Aid, (1990)
Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 1 1 4.66700 19.001 19.0
2 2 2 0 2.85800 31.272 34.0
3 3 1 1 2.43700 36.853 100.0
4 2 2 2 2.33400 38.542 9.0
5 4 0 0 2.02100 44.810 19.0
6 4 2 2 1.65010 55.656 8.0
7 5 1 1 1.55570 59.359 29.0
8 4 4 0 1.42900 65.238 34.0
9 5 3 1 1.36640 68.630 2.0
10 6 2 0 1.27820 74.119 2.0
11 5 3 3 1.23280 77.341 7.0
12 6 2 2 1.21870 78.406 4.0
13 4 4 4 1.16680 82.627 2.0
14 7 1 1 1.13200 85.762 1.0
15 6 4 2 1.08020 90.977 3.0
16 7 3 1 1.05240 94.100 9.0
17 8 0 0 1.01050 99.334 3.0
18 6 6 0 0.95270 107.908 2.0
19 7 5 1 0.93340 111.230 6.0
20 6 6 2 0.92730 112.340 2.0
21 8 4 0 0.90380 116.923 2.0
Stick Pattern
作者: 纳米镍粉 发布日期: 2008-05-29
Name and formula
Reference code: 00-043-1003
PDF index name: Cobalt Oxide
Empirical formula: Co3O4
Chemical formula: Co3O4
Crystallographic parameters
Crystal system: Cubic
Space group: Fd-3m
Space group number: 227
a (?): 8.0840
b (?): 8.0840
c (?): 8.0840
Alpha (°): 90.0000
Beta (°): 90.0000
Gamma (°): 90.0000
Calculated density (g/cm^3): 6.05
Volume of cell (10^6 pm^3): 528.30
Z: 8.00
RIR: 4.30
Subfiles and Quality
Subfiles: Inorganic
Alloy, metal or intermetalic
Corrosion
Quality: Calculated (C)
Comments
General comments: Calculation of diffractometer peak intensities done with MICRO-POWD v. 2.2 (D. Smith and K. Smith) using default instrument broadening function (NBS Table), diffracted beam monochromator polarization correction, and atomic scattering factors corrected for anomalous dispersion. Cell parameters from 9-418. Atomic positions from Roth, W., J. Phys. Chem. Solids, 25 1-10 (1964): Co(1) in 8a, Co(2) in 16d, O in 32e with x=.3881. Isotropic thermal parameters from same source: Co(1), Co(2), and O, B=.413.
References
Primary reference: Grier, D., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA., ICDD Grant-in-Aid, (1991)
Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 1 1 4.66700 19.001 16.0
2 2 2 0 2.85800 31.272 33.0
3 3 1 1 2.43740 36.846 100.0
4 2 2 2 2.33370 38.547 9.0
5 4 0 0 2.02100 44.810 20.0
6 3 3 1 1.85460 49.082 1.0
7 4 2 2 1.65010 55.656 9.0
8 5 1 1 1.55580 59.355 32.0
9 4 4 0 1.42910 65.233 38.0
10 5 3 1 1.36640 68.630 1.0
11 4 4 2 1.34730 69.743 1.0
12 6 2 0 1.27820 74.119 3.0
13 5 3 3 1.23280 77.341 8.0
14 6 2 2 1.21870 78.406 4.0
15 4 4 4 1.16680 82.627 2.0
16 5 5 1 1.13200 85.762 1.0
17 6 4 2 1.08030 90.966 4.0
18 7 3 1 1.05240 94.100 11.0
19 8 0 0 1.01050 99.334 4.0
20 7 3 3 0.98760 102.516 1.0
21 6 4 4 0.98030 103.586 1.0
22 8 2 2 0.95270 107.908 2.0
23 7 5 1 0.93350 111.212 7.0
24 6 6 2 0.92730 112.340 2.0
25 8 4 0 0.90380 116.923 3.0
26 9 1 1 0.88730 120.486 1.0
27 8 4 2 0.88200 121.702 1.0
28 6 6 4 0.86180 126.716 1.0
29 9 3 1 0.84740 130.739 6.0
30 8 4 4 0.82510 138.001 10.0
Stick Pattern
作者: simonzrh 发布日期: 2008-05-30
问题已经解决
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